FD-50F Series Pilot Freeze Drying Machine, Automatic Lyophilizer, 10kg/24hours, 0.5m2

FD-50F Series automatic freeze dryer lyophilizer, laboratory freeze dryer, pilot lyophilizer, in-situ silicone oil-heating.

PRODUCT MODEL: FD-50F Series Category: Tags: , ,

Pilot Freeze Drying Machine Description:

FD-50F freeze dryer is which freeze dried in situ (Patented product).It changes the traditional complicated operation, prevents the pollution of the material realizes the dry sublimation automation. It’s suitable for unit production.The freeze dryer has heating shelf and programmable function. It may remember freeze drying curve so the users can observe this freeze-drying process of material.

PILOT FREEZE DRYER SYSTEM

REFRIGERATION SYSTEM

                   

  • Dual-stage cooling technology easy to maintained.
  • Famous brand hermetic compressor like Tecumseh (France brand) and DANFOSS (Sweden brand), low noise, and ensure powerful cooling performance.
  • Danfoss brand of pressure controller and valve to ensure high stability.
  • Condenser -86°C for silicone oil machine, -60°C for electric heating machine. fast cooling from +20℃ to -40℃ within 30 min.
  • Shelf temperature  between -50°C to +70°C ±1°C (when it balance), Fast cooling from +20℃ to -40℃ within 60 min.
  • Air-cooled machine can be work in the room without additional cooling device.
  • Used CFC-FREE environmental-friendly refrigerant.
  • Brazed plate heat exchanger.

DRY CHAMBER

  • Rectangular type dry chamber, Pre-freezing, drying in same chamber without any manual operation.
  • Drying chamber & shelves made by polished SS 304 or material contact parts SS316 is optional, adopted high strength, high transmittance plexiglass door, easy to observe, inside round corner, easy to clean.
  • Roughness ≤ 0.6μm of inner wall of dry chamber and shelves,  flatness of shelves ≤ ±0.5mm / m to ensure best drying performance.
  • Shelf temperature  between -50°C to +70°C ±1°C (when it balance), Fast cooling from +20℃ to -40℃ within 60 min.
  • Oil circulation heating type with high temperature precision control, usually suitable for medical, bio field, electric heating type suitable for food field.
  • Shelves heating system uses safe voltage, while heating rate controllable, shelf made of mirror polish stainless steel, each shelf should be tested their roughness and flatness by professional tester in order to provide uniformity temperature for sample.
  • Wall-cross type is optional to meets with GMP standard.

CONDENSER (COLD TRAP)

  • Large capacity condenser design, made by SS304 material, SS316 is optional for the material which has high corrosivity.
  • Lowest condenser temperature reach up to -86°C for silicone oil machine, -60°C for electric heating machine.
  • Fast cooling from +20℃ to -40℃ within 30 min.
  • Independent Cylinder-type cold trap (FD-20F, FD-30F-TP, FD-50F-TP, FD-100F, FD-200), with high transmittance plexiglass door, powerful ice remove capacity to ensure best performance. Cooling pipe condenser for FD-10F, FD-30F-RE, FD-50F-RE, FD-50F-R model.
  • Patented gas diversion technology, cold trapping ice even, ice-catching ability.
  • Electric heating around the condenser chamber to remove ice effective.

CIRCULATION SYSTEM

                   

  • GUNDFOS (Denmark brand) shielded circulating pump and PID control electric heating component; circulation liquid used Low-temperature low- viscosity silicone oil.
  • Circulation system is for FD-20F, FD-30F-TP, FD-50F, FD-100F, FD-200F series.

FD-LYO CONTROL SYSTEM

  • Flexible manual + Auto control, manual groping process, auto batch production.
  • PLC control with 7’ LCD touch graphic display, can be operated in auto, semi-auto and manual mode. (Siemens brand PLC + 10’’ touch screen is optional)
  • Shelf temperature adjustable, controllable, explore suitable for pilot and production processes.
  • 32 programs, each program can be set as 36 segments, curve can be stored, processing parameters can be modified in real time.
  • Built with recorder, with USB interface data can be exported to computer for analysis, FD-LYO software & computer is optional for controlling by remote way.
  • sensor calibration function, to ensure long-term use of the accuracy of the measured value.
  • Real-time alarm display and historical alarm inquiry function, convenient fault diagnosis and equipment maintenance.
  • Users can set the level and password, decentralized operation and management.
  • WIFI Remote control software by computer or APP in mobile, you can set the machine in anywhere of the world. (Optional)

VACUUM SYSTEM

  • Two-stage rotary vane vacuum pump, vacuum is automatic adjust and can be set (optional).
  • Ultimate vacuum can reach 1 Pa, in order to reach highest vacuum, LEYBOLD/ULVAC/Edwards brand vacuum pump is optional.
  • Pump performance from atmosphere to 10 Pa less than 30 min.
  • System leaking rate less than 10 Pa·l / sec

SAFETY PROTECTION

  • Whole machine protection.
  • Operation protection like electrical system have logic interlock, control and protection function.
  • Alarm for vacuum system, heating system and etc.
  • Power off/on protection, sublimation process protection
  • Material protection during sublimation process, Heat cutting if vacuum lack
  • Condenser-vacuum system interlock protection system.

OTHER FEATURES

  • Normal type suitable for bulk raw products like food, fruit, herbal medicine and bio material. Stoppering type suitable for vials comes with cap, to stoppering caps into the vials.
  • Inflatable (water) valve with a safety diaphragm valve can be connected to the inert gas source, dry and filled with inert gas, to extend the shelf life of the material.
  • CE/ISO 9001 13485 14001 certificated, can be conforms to GMP standard as per customer’s requirements

MAIN COMPONENTS LIST

OPTIONAL LIST

SPECIFICATIONS

FD-50F Series

Model

FD-50F-RE

FD-50F-R

FD-50F-TP

Heating type

Electric heating

Silicone oil circulation

Silicone oil circulation

Picture

Drying chamber

Freeze-drying area

0.6 m2

0.7 m2

0.5 m2

Shelf quantity

6 pcs

4+1 pcs

3+1 pcs

Shelf temp. range

-50°C ~70°C

-50°C ~70°C

-50~70°C

Temp. Difference

+/-1°C (balance)

+/-1°C (balance)

+/-1°C (balance)

Shelf size

300×340mm

480×360mm

410×410mm

Shelf spacing

50mm

50mm

70mm

Sample load capacity

6L

7L

5L

Tray quantity

6 pcs

4 pcs

3 pcs

Tray size

295×335mm

475×355mm

405×405mm

Vial load capacity

Ф22 vials (piece)

1408

1408

1050

Ф16 vials (piece)

2728

2728

2058

Ф12vials (piece)

4920

4920

3705

Cold trap

Cold trap temperature

≤-60°C

≤-75°C

≤-75°C

Ice capture capability

10 Kg/24h

10 Kg/24h

10 Kg/24h

Electric defrost

Nature

Nature

Electric or hot gas

Cool type

Air cooled

Air cooled

Air cooled

Basic parameters

Style of top-press

Hydraulic pressure

Ultimate vacuum

≤5Pa

≤5Pa

≤5Pa

Vacuum pump

Included

Included

Included

Pump rate

8L/S

8L/S

8L/S

Dimension (mm)

890 × 670 × 1410

1000 × 785 × 1420

1490 × 850 × 1620 + 240

Weight

450kg

600kg

800 kg

Voltage Freeze dryer

380V±10%

50Hz/60Hz

380V±10%

50Hz/60Hz

380V±10%

50Hz/60Hz

Power

4500W

5500W

6500W


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