Labfreez FD-20F-R Pilot Freeze Dryer Operation Video

FD-20F electric-heating freeze dryer is freeze-dried in situ. It changes the traditional complicated operation, prevents the pollution of the material and realizes the dry sublimation automation.
The freeze dryer has heating and programmable function. It may remember freeze drying curve so the users can observe freeze-drying process of material.

PILOT FREEZE DRYER SYSTEM

FD-30F-E electric-heating freeze dryer is freeze-dried in situ. It changes the traditional complicated operation, prevents the pollution of the material and realizes the dry sublimation automation. The freeze dryer has heating and programmable function. It may remember freeze drying curve so the users can observe freeze-drying process of material.

REFRIGERATION SYSTEM

                   

  • Dual-stage cooling technology easy to maintained.
  • Famous brand hermetic compressor like Tecumseh (France brand) and DANFOSS (Sweden brand), low noise, and ensure powerful cooling performance.
  • Danfoss brand of pressure controller and valve to ensure high stability.
  • Condenser -86°C for silicone oil machine, -60°C for electric heating machine. fast cooling from +20℃ to -40℃ within 30 min.
  • Shelf temperature  between -50°C to +70°C ±1°C (when it balance), Fast cooling from +20℃ to -40℃ within 60 min.
  • Air-cooled machine can be work in the room without additional cooling device.
  • Used CFC-FREE environmental-friendly refrigerant.
  • Brazed plate heat exchanger.

DRY CHAMBER

  • Rectangular type dry chamber, Pre-freezing, drying in same chamber without any manual operation.
  • Drying chamber & shelves made by polished SS 304 or material contact parts SS316 is optional, adopted high strength, high transmittance plexiglass door, easy to observe, inside round corner, easy to clean.
  • Roughness ≤ 0.6μm of inner wall of dry chamber and shelves,  flatness of shelves ≤ ±0.5mm / m to ensure best drying performance.
  • Shelf temperature  between -50°C to +70°C ±1°C (when it balance), Fast cooling from +20℃ to -40℃ within 60 min.
  • Oil circulation heating type with high temperature precision control, usually suitable for medical, bio field, electric heating type suitable for food field.
  • Shelves heating system uses safe voltage, while heating rate controllable, shelf made of mirror polish stainless steel, each shelf should be tested their roughness and flatness by professional tester in order to provide uniformity temperature for sample.
  • Wall-cross type is optional to meets with GMP standard.

CONDENSER (COLD TRAP)

  • Large capacity condenser design, made by SS304 material, SS316 is optional for the material which has high corrosivity.
  • Lowest condenser temperature reach up to -86°C for silicone oil machine, -60°C for electric heating machine.
  • Fast cooling from +20℃ to -40℃ within 30 min.
  • Independent Cylinder-type cold trap (FD-20F, FD-30F-TP, FD-50F-TP, FD-100F, FD-200), with high transmittance plexiglass door, powerful ice remove capacity to ensure best performance. Cooling pipe condenser for FD-10F, FD-30F-RE, FD-50F-RE, FD-50F-R model.
  • Patented gas diversion technology, cold trapping ice even, ice-catching ability.
  • Electric heating around the condenser chamber to remove ice effective.

CIRCULATION SYSTEM

                   

  • GUNDFOS (Denmark brand) shielded circulating pump and PID control electric heating component; circulation liquid used Low-temperature low- viscosity silicone oil.
  • Circulation system is for FD-20F, FD-30F-TP, FD-50F, FD-100F, FD-200F series.

FD-LYO CONTROL SYSTEM

  • Flexible manual + Auto control, manual groping process, auto batch production.
  • PLC control with 7’ LCD touch graphic display, can be operated in auto, semi-auto and manual mode. (Siemens brand PLC + 10’’ touch screen is optional)
  • Shelf temperature adjustable, controllable, explore suitable for pilot and production processes.
  • 32 programs, each program can be set as 36 segments, curve can be stored, processing parameters can be modified in real time.
  • Built with recorder, with USB interface data can be exported to computer for analysis, FD-LYO software & computer is optional for controlling by remote way.
  • sensor calibration function, to ensure long-term use of the accuracy of the measured value.
  • Real-time alarm display and historical alarm inquiry function, convenient fault diagnosis and equipment maintenance.
  • Users can set the level and password, decentralized operation and management.
  • WIFI Remote control software by computer or APP in mobile, you can set the machine in anywhere of the world. (Optional)

VACUUM SYSTEM

  • Two-stage rotary vane vacuum pump, vacuum is automatic adjust and can be set (optional).
  • Ultimate vacuum can reach 1 Pa, in order to reach highest vacuum, LEYBOLD/ULVAC/Edwards brand vacuum pump is optional.
  • Pump performance from atmosphere to 10 Pa less than 30 min.
  • System leaking rate less than 10 Pa·l / sec

SAFETY PROTECTION

  • Whole machine protection.
  • Operation protection like electrical system have logic interlock, control and protection function.
  • Alarm for vacuum system, heating system and etc.
  • Power off/on protection, sublimation process protection
  • Material protection during sublimation process, Heat cutting if vacuum lack
  • Condenser-vacuum system interlock protection system.

OTHER FEATURES

  • Normal type suitable for bulk raw products like food, fruit, herbal medicine and bio material. Stoppering type suitable for vials comes with cap, to stoppering caps into the vials.
  • Inflatable (water) valve with a safety diaphragm valve can be connected to the inert gas source, dry and filled with inert gas, to extend the shelf life of the material.
  • CE/ISO 9001 13485 14001 certificated, can be conforms to GMP standard as per customer’s requirements

MAIN COMPONENTS LIST

OPTIONAL LIST

SPECIFICATIONS

FD-20F Series

Model

FD-20F-R

FD-20F-TP

Specification

Normal

With stoppering

Pictures

Drying chamber

Freeze-drying area

0.3 m2

0.2 m2

Heating method

Circulation oil heating

Circulation oil heating

Shelf’s quantity

3 pcs

2+1 pcs

Shelves temp. range

-50°C ~70°C

-50°C ~70°C

Temp. difference

1°C

1°C

Shelf’s distance

70mm

70mm

Dimensions of shelves

400*270 mm

400*270 mm

Size of tray

395×265mm * 3 pcs

395×265mm * 2 pcs

Sample loaded capacity

3L

3L

Stoppering device

Manual

Material

SS304 (chamber, shelves, trays)

SS304 (chamber, shelves, trays)

Vials load capacity (pcs)

Ф22 vials

440

440

Ф16 vials

868

868

Ф12 vials

1554

1554

Cold trap

Lowest temperature

≤ -85°C

≤ -85°C

Water-capture capability

6 Kg/24h

6 Kg/24h

Material

SS304

SS304

Condenser size (D*H)

Ф195×470mm

Ф195×470mm

Volume

40L

40L

Basic parameters

Ultimate Vacuum

≤5 Pa

≤5 Pa

Vacuum pump

2XZ-4

2XZ-4

Pump rate

4L/s

4L/s

Cooling method

Air cooled

Air cooled

Power supply

220V/50Hz or 110V/60Hz

220V/50Hz or 110V/60Hz

Power

3000W

3000W

Weight

300kg

310kg

Dimension

770x750x1520 mm

770x750x1650 mm

Control method

PLC auto + manual

PLC auto + manual

Operation Video

Labfreez FD-20F-R Pilot Freeze Dryer Operation Video