FD-200F Pilot Freeze Dryer lyophilizer Machine, 40kg/24hours, 2 square meter

  • 2m2 shelf area, 20kg~30kg/batch, 40kg/24hr ice remove capacity
  • High precision thermal oil circulating temperature control method
  • Automatic + manual operation, remote control by computer
  • France Origined famous brand compressor, circulating pump, pressure gauge
  • Air cooled no need of external cooling water source
  • Works for food, bio samples, medicine, vaccine vial, microplate
  • CE/ISO9001, GMP

FD-200F Series pilot freeze drying machine is suitable for freeze-drying of bulk (liquid, paste, solid) conventional substances, but also suitable for drying of vials. When preparing for freeze-drying, the materials are divided into vials as needed, and the bottle caps are floated and then frozen. Drying. After drying, operate the capping device to tighten the bottle cap, which can avoid secondary pollution and re-adsorption of moisture, making it easy to store for a long time.

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REFRIGERATION SYSTEM

  • Dual-stage cooling technology easy to maintained.
  • Famous brand hermetic compressor like Tecumseh (France brand) and DANFOSS (Sweden brand), low noise, and ensure powerful cooling performance.
  • Danfoss brand of pressure controller and valve to ensure high stability.
  • Condenser -86°C for silicone oil machine, -60°C for electric heating machine. fast cooling from +20℃ to -40℃ within 30 min.
  • Shelf temperature  between -50°C to +70°C ±1°C (when it balance), Fast cooling from +20℃ to -40℃ within 60 min.
  • Air-cooled machine can be work in the room without additional cooling device.
  • Used CFC-FREE environmental-friendly refrigerant.
  • Brazed plate heat exchanger.

                   

 

 

DRY CHAMBER

  • Rectangular type dry chamber, Pre-freezing, drying in same chamber without any manual operation.
  • Drying chamber & shelves made by polished SS 304 or material contact parts SS316 is optional, adopted high strength, high transmittance plexiglass door, easy to observe, inside round corner, easy to clean.
  • Roughness ≤ 0.6μm of inner wall of dry chamber and shelves,  flatness of shelves ≤ ±0.5mm / m to ensure best drying performance.
  • Shelf temperature  between -50°C to +70°C ±1°C (when it balance), Fast cooling from +20℃ to -40℃ within 60 min.
  • Oil circulation heating type with high temperature precision control, usually suitable for medical, bio field, electric heating type suitable for food field.
  • Shelves heating system uses safe voltage, while heating rate controllable, shelf made of mirror polish stainless steel, each shelf should be tested their roughness and flatness by professional tester in order to provide uniformity temperature for sample.
  • Wall-cross type is optional to meets with GMP standard.

 

 

CONDENSER (COLD TRAP)

  • Large capacity condenser design, made by SS304 material, SS316 is optional for the material which has high corrosivity.
  • Lowest condenser temperature reach up to -86°C for silicone oil machine, -60°C for electric heating machine.
  • Fast cooling from +20℃ to -40℃ within 30 min.
  • Independent Cylinder-type cold trap (FD-20F, FD-30F-TP, FD-50F-TP, FD-100F, FD-200), with high transmittance plexiglass door, powerful ice remove capacity to ensure best performance. Cooling pipe condenser for FD-10F, FD-30F-RE, FD-50F-RE, FD-50F-R model.
  • Patented gas diversion technology, cold trapping ice even, ice-catching ability.
  • Electric heating around the condenser chamber to remove ice effective.

 

 

CIRCULATION SYSTEM

  • GUNDFOS (Denmark brand) shielded circulating pump and PID control electric heating component; circulation liquid used Low-temperature low- viscosity silicone oil.
  • Circulation system is for FD-20F, FD-30F-TP, FD-50F, FD-100F, FD-200F series.

                   

 

 

FD-LYO CONTROL SYSTEM

  • Flexible manual + Auto control, manual groping process, auto batch production.
  • PLC control with 7’ LCD touch graphic display, can be operated in auto, semi-auto and manual mode. (Siemens brand PLC + 10’’ touch screen is optional)
  • Shelf temperature adjustable, controllable, explore suitable for pilot and production processes.
  • 32 programs, each program can be set as 36 segments, curve can be stored, processing parameters can be modified in real time.
  • Built with recorder, with USB interface data can be exported to computer for analysis, FD-LYO software & computer is optional for controlling by remote way.
  • sensor calibration function, to ensure long-term use of the accuracy of the measured value.
  • Real-time alarm display and historical alarm inquiry function, convenient fault diagnosis and equipment maintenance.
  • Users can set the level and password, decentralized operation and management.
  • WIFI Remote control software by computer or APP in mobile, you can set the machine in anywhere of the world. (Optional)

 

 

 

VACUUM SYSTEM

  • Two-stage rotary vane vacuum pump, vacuum is automatic adjust and can be set (optional).
  • Ultimate vacuum can reach 1 Pa, in order to reach highest vacuum, LEYBOLD/ULVAC/Edwards brand vacuum pump is optional.
  • Pump performance from atmosphere to 10 Pa less than 30 min.
  • System leaking rate less than 10 Pa·l / sec

 

 

SAFETY PROTECTION

  • Whole machine protection.
  • Operation protection like electrical system have logic interlock, control and protection function.
  • Alarm for vacuum system, heating system and etc.
  • Power off/on protection, sublimation process protection
  • Material protection during sublimation process, Heat cutting if vacuum lack
  • Condenser-vacuum system interlock protection system.

 

 

OTHER FEATURES

  • Normal type suitable for bulk raw products like food, fruit, herbal medicine and bio material. Stoppering type suitable for vials comes with cap, to stoppering caps into the vials.
  • Inflatable (water) valve with a safety diaphragm valve can be connected to the inert gas source, dry and filled with inert gas, to extend the shelf life of the material.
  • CE/ISO 9001 13485 14001 certificated, can be conforms to GMP standard as per customer’s requirements

 

MAIN FEATURES

 

 

MAIN COMPONENTS LIST

 

 

SPECIFICATIONS OF FREEZE DRYING MACHINE

FD-200F Series

Model

FD-200F-R

FD-200F-TP

Heating type

Silicone oil circulation

Silicone oil circulation

 

Picture

FD-200F-R pilot food freeze dryer, 20kg lyophilizer

FD-200F-TP pilot vaccine freeze dryer, 20kg lyophilizer

Drying chamber

Freeze-drying area

2.25 m2

1.98 m2

Shelves quantity

5+1pcs

4+1pcs

Shelf Temperature

-50°C ~70°C

-50°C ~70°C

Shelf Temp. Accuracy

± 1°C (when stable)

± 1°C (when stable)

Shelf spacing

80mm

100mm

Size of shelves

500*900*20 mm

610*810*20 mm

Raw material load capacity (be better)

22L (when thickness 10mm)

20L (when thickness 10mm)

Material of chamber

Polish SS304

Polish SS304

Material of Shelves

Polish SS304

 Polish SS304

Material of trays

SS304

SS304

Tray quantity

10 pcs

16 pcs

Stoppering device

–

Hydraulic pressure

Vials load capacity

Ф22 vials (PCS)

4100

3600

Ф16 vials (PCS)

7800

6800

Ф12 vials (PCS)

14400

12600

Condenser

Max temperature

≤-85°C (Empty load)

≤-85°C (Empty load)

Water-capture capability

30 Kg/24h

30 Kg/24h

Defrost

water soaking

water soaking

Material

SS304 or SS316 (Optional)

SS304 or SS316 (Optional)

Basic parameters

Vacuum degree

≤5 Pa

≤5 Pa (Range:1~300Pa)

Dimension

1200*2100*1700 (mm)

2100x1400x2400 (mm)

Max Power

13.5kw

15.5kw

Weight

1200 kg

1500 kg

Data Process

RS232 Interface or USB

Control method

PLC auto + manual

Refrigeration unit

Compressor

Bitzer or TECUMSEH, 2 set

Power

7 Kw

Refrigerant

R507 & R23

Cooling type

Air cooled

Pressure controller

DANFOSS

Expansion valve

DANFOSS

 

OPTIONAL LIST

Item No.

Item Name

FDF1001

Mobile remote control (Iphone or Android APP support)

FDF1002

Control computer software

FDF1003

Laptop

FDF1004

Eutectic point tester

FDF1005

Ulvac(Japan) Vacuum Pump/ Leybold(Germany)

FDF1006

Condenser defrost device (for FD-10F, FD-20F, FD-30F-RE, FD-30F-R, FD-50F-RE, FD-50F-R)

FDF1007

Air compressor (for Pneumatic door opening)

FDF1008

Vacuum pump solenoid control valve

FDF1009

External material change to SS304

FDF1010

Condenser, trays, shelves change to SS316

FDF1011

4 port Tree type manifold system (extra port customizable)

FDF1012

6 port Tree type manifold system (extra port customizable)

FDF1013

Extra set of trays

FDF1014

Chamber condenser isolation valve

FDF1015

Oil mist filter for vacuum pump

FDF1017

Oil anti-back valve for vacuum pump

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