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FD-10F series In-situ Freeze Dryer, Laboratory Vacuum Lyophilization Machine
FD-10F series is the most compact type of Pilot Freeze Dryer Machine, it is a automatic type which the samples can be pre-freezing and drying in same chamber, this series is suitable for small batch process for bio samples, probiotics, polypeptide, pharmaceutical, vaccine in vials, traditional medince, food, fruit and etc. There are severals models of FD-10F series:
- FD-10F-R silicone oil circulating heating and cooling shelf temperature control
- FD-10F-RE electric heating and refrigeration flow to shelf to cooling
- FD-10F-TP similar with FD-10F-R and comes with stoppering device for sealing rubber caps into vials under vacuum
- FD-10F-TPE similar with FD-10F-RE and comes with stoppering device for sealing rubber caps into vials under vacuum
Chamber
- Rectangular type dry chamber, Pre-freezing, drying in same chamber without any manual operation.
- Drying chamber & shelves made by polished SS 304 or material contact parts SS316 is optional, adopted high strength, high transmittance plexiglass door, easy to observe, inside round corner, easy to clean.
- Oil circulation heating type with high temperature precision control, usually suitable for medical, bio field, electric heating type suitable for food field.
- GUNDFOS shielded circulating pump and PID control electric heating component; circulation liquid used Low-temperature low- viscosity silicone oil.
- Shelves heating system uses safe voltage, while heating rate controllable. (Electric heating type)
Condenser Chamber (cold trap)
- Large capacity condenser design, made by SS304 material, SS316 is optional for the material which has high corrosivity.
- Lowest condenser temperature reach up to -86°Cfor silicone oil machine, -60°C for electric heating machine.
- Fast cooling from +20°C to -40°C within 30 min.
- Independent Cylinder-type cold trap, with high transmittance plexiglass door, powerful ice remove capacity to ensure best performance.
- Patented gas diversion technology, cold trapping ice even, ice-catching ability.
- Electric heating around the condenser chamber to remove ice effective.
Refrigeration System
- Dual-stage cooling technology easy to maintained.
- Famous brand hermetic compressor like Tecumseh (France brand) and DANFOSS (Sweden brand), low noise, and ensure powerful cooling performance.
- Danfoss brand of pressure controller and valve to ensure high stability.
- Condenser -86°Cfor silicone oil machine, -60°C for electric heating machine. fast cooling from +20°C to -40°C within 30 min.
- Shelf temperature between -50°C to +70°C ±1°C (when it balance), Fast cooling from +20°C to -40°C within 60 min.
- Air-cooled machine can be work in the room without additional cooling device.
- Used CFC-FREE environmental-friendly refrigerant.
- Brazed plate heat exchanger.
Circulation System
- GUNDFOS (Denmark brand) shielded circulating pump and PID control electric heating component; circulation liquid used Low-temperature low- viscosity silicone oil.
- Circulation system is for model FD-10F-R, FD-10F-TP silicone oil shelf temperature control.
Control System
- Flexible manual + Auto control, manual groping process, auto batch production.
- PLC control with 7’ LCD touch graphic display, can be operated in auto, semi-auto and manual mode. (Siemens brand PLC + 10’’ touch screen is optional)
- Shelf temperature adjustable, controllable, explore suitable for pilot and production processes.
- 32 programs, each program can be set as 36 segments, curve can be stored, processing parameters can be modified in real time.
- Built with recorder, with USB interface data can be exported to computer for analysis, FD-LYO software & computer is optional for controlling by remote way.
- sensor calibration function, to ensure long-term use of the accuracy of the measured value.
- Real-time alarm display and historical alarm inquiry function, convenient fault diagnosis and equipment maintenance.
- Users can set the level and password, decentralized operation and management.
- WIFI Remote control software by computer or APP in mobile, you can set the machine in anywhere of the world. (Optional)
Vacuum System
- Two-stage rotary vane vacuum pump, vacuum is automatic adjust and can be set (optional).
- Ultimate vacuum can reach 1 Pa, in order to reach highest vacuum, LEYBOLD/ULVAC brand vacuum pump is optional.
- Pump performance from atmosphere to 10 Pa less than 30 min.
- System leaking rate less than 10 Pa·l / sec
Safety Protection
- Whole machine protection.
- Operation protection like electrical system have logic interlock, control and protection function.
- Alarm for vacuum system, heating system and etc.
- Power off/on protection, sublimation process protection
- Material protectionduring sublimation process, Heat cutting if vacuum lack
- Condenser-vacuum system interlock protection system.
Other Features
- Normal type suitable for bulk raw products like food, fruit, herbal medicine and bio material. Stoppering type suitable for vials comes with cap, to stoppering caps into the vials.
- Inflatable (water) valve with a safety diaphragm valve can be connected to the inert gas source, dry and filled with inert gas, to extend the shelf life of the material.
- CE/ISO 9001 13485 14001 certificated, can be conforms to GMP standard as per customer’s requirements
Documents
Specifications of FD-10F Series lyophilization machine
| MODEL | FD-10F-R FD-10F-RE | FD-10F-TP FD-10F-TPE |
| Specification | Normal lyophilization machine | lyophilization machine with stoppering | |
| Picture |  |  | |
| Drying chamber | Shelf area | 0.2 m2 | 0.1 m2 |
| Shelf quantity | 2 pcs | 1 pc | |
| Shelf heating | Silicon oil heating Electric heating | Silicon oil heating Electric heating | |
| Shelf temp. range | -40°C ~ +70°C (Silicon oil heating) -50°C ~ +70°C (Electric heating) | ||
| Shelf space height | 70 mm | ||
| Shelf dimension | 400×270 mm | ||
| Tray dimensions | 395×265 mm | 395×265 mm | |
| Tray quantity (pcs) | 2 | 1 | |
| Sample loaded capacity | 2L (thickness 10mm) | 1L (thickness 10mm) | |
| Stoppering device | – | Manual | |
| Material | SS304 (chamber, shelves, trays, pipe) | ||
| Vials load capacity (pcs) | Ф22 vials | 440 | 220 |
| Ф16 vials | 868 | 434 | |
| Ф12 vials | 1554 | 777 | |
| Condenser | Max temp. | ≤-65°C ≤-60°C (-80°C is optional) | |
| Ice capture capacity | 6Kg/24hs | ||
| Defrost | Natural (Electric heating is optional) | ||
| Material | SS304 | ||
| Vacuum | Vacuum pump | Included | |
| Vacuum rate | 4L/S | ||
| Vacuum degree | ≤5 Pa | ||
| Basic parameters | Style of cooling | Air-cooled | |
| Dimension(L*W*H) | 655×640×1200mm | 655×640×1200mm | |
| Weight | 210kg | 210kg | |
| Control method | PLC auto + manual | ||
| Installation power | 2 Kw | ||
| Voltage | 220V/50Hz (can be change to 110V/60Hz) | ||
